4-Meth­oxy­anilinium 2-carb­oxy-4,5-di­chloro­benzoate

نویسندگان

  • Graham Smith
  • Urs D. Wermuth
چکیده

In the title salt C7H10NO(+)·C8H3Cl2O4 (-) the benzene rings of the cation and anion are essentially parallel [inter-ring dihedral angle 4.8 (2)°]. In the anion the carb-oxy-lic acid and carboxyl-ate groups make dihedral angles of 19.0 (2) and 79.5 (2)°, respectively, with the benzene ring. Aminium N-H⋯O, carb-oxy-lic acid O-H⋯O and weak aromatic C-H⋯O hydrogen-bonding associations with carboxyl O-atom acceptors together with cation-anion π-π ring inter-actions [minimum ring centroid separation = 3.734 (3) Å] give rise to a sheet structure lying parallel to (001).

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Isopropyl­aminium 2-carb­oxy-4,5-di­chloro­benzoate

In the structure of the 1:1 proton-transfer compound of isopropyl-amine with 4,5-dichloro-phthalic acid, C(3)H(10)N(+)·C(8)H(3)Cl(2)O(4) (-), the three cation H-atom donors associate with three separate carboxyl O-atom anion acceptors, giving conjoint cyclic R(4) (4)(12), R(4) (4)(16) hydrogen-bonding cation-anion inter-actions in a one-dimensional ribbon structure. In the anions, the carboxyl ...

متن کامل

4-Methyl­pyridinium 2-carb­oxy-4,5-dichloro­benzoate monohydrate

In the structure of the 1:1 proton-transfer compound of 4-methyl-pyridine (γ-picoline) with 4,5-dichloro-phthalic acid, C(6)H(8)N(+)·C(8)H(3)Cl(2)O(4) (-)·H(2)O, determined at 200 K, the 4,5-dichloro-phthalate anions are bridged by the water mol-ecule through O-H⋯O(carbox-yl) hydrogen bonds, giving zigzag chains which extend along the c-axis direction. The 4-methyl-pyridinium cations are linked...

متن کامل

4-Chloro­anilinium 2-carb­oxy-4,5-dichloro­benzoate

The structure of the 1:1 proton-transfer compound of 4-chloro-aniline with 4,5-dichloro-phthalic acid (DCPA), viz. C(6)H(7)ClN(+)·C(8)H(3)Cl(2)O(4) (-), has been determined at 130 K. The non-planar hydrogen phthalate anions and the 4-chloro-anilinium cations form two-dimensional O-H⋯O and N-H⋯O hydrogen-bonded substructures which have no peripheral extension. Between the sheets there are weak π...

متن کامل

5-Carb­oxy-1,3-bis­(carb­oxy­meth­yl)-4-imidazolinium-4-carboxyl­ate

The title compound, C(9)H(8)N(2)O(8), was obtained by the reaction of imidazole-4,5-dicarb-oxy-lic acid and 2-chloro-acetic acid. An intra-molecular O-H⋯O hydrogen bond occurs. The crystal packing is stabilized by intermolecular O-H⋯O and C-H⋯O hydrogen bonds, which link mol-ecules into a three-dimensional network.

متن کامل

tert-Butyl­aminium 2-carb­oxy-4,5-dichloro­benzoate

In the structure of the title anhydrous salt, C(4)H(12)N(+)·C(8)H(3)Cl(2)O(4) (-), the 4,5-dichloro-phthalate monoanions have the common 'planar' conformation with the carboxyl groups close to coplanar with the benzene ring and with a short intra-molecular carb-oxy-lic acid O-H⋯O hydrogen bond. In the crystal, a two-dimensional sheet structure is formed through aminium N-H⋯O(carbox-yl) hydrogen...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:

دوره 69  شماره 

صفحات  -

تاریخ انتشار 2013